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Volume 5 is the fifth volume of the Pokémon Diamond and Pearl Adventure! manga. Authored and illustrated by 伊原しげかつ Shigekatsu Ihara.
- Hareta breaks through to Mitsumi, freeing her from Team Galactic's influence.
- Cyrus forms the Red Chain.
- Jun saves Hareta and Mitsumi from the self-destructing Team Galactic HQ.
- Piplup evolves into Empoleon.
- Hareta and Jun head to Mt. Coronet where Cyrus has summoned Dialga.
- Palkia also appears and wars against Dialga.
- With everyone's help, the gods are quelled and Cyrus learns the error of his ways.
The following Pokémon evolve:
- As the English volumes do not have dust covers like the Japanese ones, part two of the back cover gag is lost in the English release. The front cover image is moved to the end of the volume and changed into an explanation of the direction the book reads in.